Tuesday, May 8, 2012

Solid State NMR lab


We are trying to get the word out about a relatively new and unique service here at KU - a regional solid state NMR lab. 

The KU Solid State NMR facility specializes in the analysis of solid materials. Projects come from a wide variety of fields including soils, pharmaceutics, biomass, catalysts, biological materials, organometallics, and inorganics. The lab is equipped with a Bruker Avance III three-channel spectrometer and two probes.

The primary probe is a Multiple Sample Solids probe from Revolution, NMR (Ft. Collins, CO). This probe has four independent circuits in it that can be operated simultaneously. Two of those circuits are equipped with 7 mm spinning modules, one has a 2.5 mm spinning module, and one has a 4 mm spinning system. The 4 mm system has HXY triple resonance capability. The other three circuits are HX circuits. The X and Y channels of all four circuits can work with nuclei ranging from 15N to 31P.

The second probe is a Bruker (Billerica, MA) 4mm two channel (HX) probe. It has variable temperature capabilities from -50 C to + 80 C.

Inquiries regarding use of the facility should be directed to:
Dewey Barich, Solid State NMR Facility
dhbarich@ku.edu
785-864-4719
2095 Constant Ave.
Lawrence, KS 66047

 Also see the website at ...

http://kunmr-suse.msg.ku.edu/ssnmr.html

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